How to make nitrous oxide

• Author: admin
• Filed under: Uncategorized
• Date: Feb 7,2008

From this article you will learn how to make nitrous oxide.

Ingredients to make nitrous oxide:
REMEMBER: use exact quantities written here.

• Ammonium Nitrate (NH4NO3) - get a good grade, it’s a fertilizer and comes in 50lb. bags.

• Clean sand. Fairly fine grained (30 mesh or finer.)

• Electric hot plate (500 to 2500 watt) with variable heat.

• Stainless steel dial thermometer. (This is the only metal item which may be used.) It must go to 250 C (450 F). Select the Erlenmeyer flask (next item) and the thermometer so that the thermometer can reach at least within 1/16″ of the bottom of the flask through the stopper.

• A 2000 to 4000 ml PYREX or KIMAX Erlenmeyer flask.

• Several feet of 3/8″ clear vinyl or surgical rubber tubing.

• At least 4 8mm ID glass or plastic tubing “T’s”.

• 1 120 degree bend 8mm ID PYREX glass elbow, with about 3″ of tubing on each side of the bend.

• 7 6-8″ long pieces of 8mm ID glass or plastic tubing.

• 3 6-8 feet long 1.5″ to 2″ diameter glass or clear plastic pipes.

• 1 two hole rubber or neoprene stopper to fit the top of the Erlenmeyer flask. One hole should fit the 8mm ID PYREX glass elbow, and the other hole should fit the stainless steel dial thermometer.

• 6 one hole rubber or neoprene stoppers that will fit the ends of the clear plastic or glass pipes. The holes in the stoppers must fit the straight 8mm ID glass or plastic tubes.

• NH4 NO3 ———————-> N2O2 + 2*H2O

• Ammonium Nitrate ———————-> nitrous oxide + two water

Asembly

NOTE: When inserting tubing through stopper holes, ALWAYS WRAP AND HOLD THE TUBING WITH A CLOTH. Also moisten the tip of the tubing and the stopper hole with glycerin, soap, or spit. (never oil)

• Into the stopper with two holes, inset the thermometer far enough so that when the stopper is put into the Erlenmeyer flask, it almost touches the bottom of the flask (but don’t allow it to touch), and then insert one end of the glass elbow far enough through the stopper so that it sticks out 1/4″ to 1/2″.

• Into the six one-hole stoppers, insert a piece of the 8mm ID glass (or plastic) tubing so that 1/2″ to 3/4″ protrudes from the narrow end of the stopper.

• Now select your set-up space so that there is 1.5 feet of space clear in all directions around the hotplate, so that the three scrubber pipes can lie side by side where they will not be knocked over.

• Take approximately 2 feet of the 3/8″ flexible tubing and connect one end to the glass elbow in the two-hole stopper, and the other end to the middle of one of the 8mm ID glass (or hard plastic) “T’s”.

• With short pieces (select lengths for a neat fit) of 3/8″ tubing and another 8mm “T” assemble the INLET SET manifold and connect it to the bottom end of the scrubbers. Stoppers may then be inserted into the lower end of the scrubber pipes.

• Elevate the OUT end of the scrubber pipes so that the upper end is 6″ to 8″ above the IN end, but no more, and then fill the pipes with water until they are full within 4″ to 8″ of the top (outlet) end, and insert the outlet stoppers. Try to fill all the scrubbers equally full.

• With short pieces of 3/8″ tubing and two 8mm ID “T’s”, prepare and connect the OUTLET SET manifold to the scrubbers similar to the way the set was connected in step 5.

• To the last “T” of the OUTLET SET (of “T’s” manifold), connect a fairly long piece of 3/8″ tubing to reach a “safe” location (where connection and disconnection of the receiver bags will not disturb the scrubbers) and secure it. Then put the last piece of 8mm ID hard tubing into the free end.

• Finally, prepare several receiever bags by inserting about an 8″ piece of tubing into the top so that 3″ or 4″ sticks out of the bag and secure it in place with a rubber band.

Congratulations !!! Now you have your own nitrous oxide generator.